HCID 21961332, compound → HCID 15516561, compound

HRID 272329Notes

Reaction equation

HRID 272329 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[C:12]3[C:13]([CH3:30])=[C:14]([N:19]4[C:27](=O)[C:26]5[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=5)[C:20]4=O)[C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][C:9]2([CH3:32])[CH3:31])=[CH:4][CH:3]=1>C(OCC)(=O)C>[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[C:12]3[C:13]([CH3:30])=[C:14]([N:19]4[CH2:20][C:21]5[C:26](=[CH:25][CH:24]=[CH:23][CH:22]=5)[CH2:27]4)[C:15]([CH3:18])=[C:16]([CH3:17])[C:11]=3[O:10][C:9]2([CH3:32])[CH3:31])=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 21961332HCID 21961332, compound

Product 1

HCID 15516561HCID 15516561, compoundYield 55%

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

By using 2-[3-(4-fluorophenyl)-2,2,4,6,7-pentamethyl-2,3-dihydro-1-benzofuran-5-yl]-1H-isoindole-1,3(2H)-dione, the title compound was synthesized according to Example 2a. Yield: 55%. Melting point: 204-205° C. (Ethyl acetate)

Sources & evidence

ORD record
ord-d4c39a8f288f4552b8f134b4b319bd8f
Source dataset
uspto-grants-2008_11
Patent number
US07456162B2

Reaction notes

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