HRID272364

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID67879

Benzoyl chloride, 4-fluoro-

C7H4ClFO

结构：Cc1c(C)c2c(c(C)c1N)C(c1ccccc1)C(C)(C)O2

HCID10540798

未命名化合物

PRODUCTS

生成物

结构：Cc1c(C)c2c(c(C)c1NC(=O)c1ccc(F)cc1)C(c1ccccc1)C(C)(C)O2

HCID10294590

未命名化合物

收率 92%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

By using 2,2,4,6,7-pentamethyl-3-phenyl-2,3-dihydro-1-benzofuran-5-amine and 4-fluorobenzoyl chloride, the title compound was synthesized according to Example 1b. Yield: 92%. Melting point: 156-158° C. (Ethyl acetate)