HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine, 1-cyclopentyl-4-(4-nitro-2-pyridinyl)- → HCID 62367922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine, 1-cyclopentyl-4-(4-nitro-2-pyridinyl)- | HCID 51105608 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 62367922 | HCID 62367922 | 95% |
Reaction Steps
A mixture of 2.85 g (10 mmol) 1-cyclopentyl-4-(4-nitro-pyridin-2-yl)-piperazine and 0.285 g Pd/C (10%) in 25 ml methanol was treated with 1 bar hydrogen at room temperature for 3 h. After filtration the mixture was evaporated to dryness to yield 2.34 g (92%) of the title compound as brownish solid. (m/e): 247.4 (MH+; 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456175B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-c6a40dfee73b4fb88f7cd0ea0f65896c |
| Source note | uspto-grants-2008_11 |