HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylhydrazine → 3-tert-Butyl-3,4,9-triaza-tricyclo[5.3.1.0 2,6]undeca-2(6),4-diene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylhydrazine | HCID 81890 | — |
| Reactant | 3-Benzyl-7-dimethylaminomethylene-3-aza-bicyclo[3.2.1]octan-6-one | HCID 68808337 | — |
| Product | 3-tert-Butyl-3,4,9-triaza-tricyclo[5.3.1.0 2,6]undeca-2(6),4-diene | HCID 68807084 | — |
Reaction Steps
Following the method described in Example 14, 3-benzyl-7-dimethylaminomethylene-3-aza-bicyclo[3.2.1]octan-6-one and t-butyl hydrazine were converted to the title compound in 7.5% overall yield. APCl MS m/z 206.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456177B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-936d041243f34af0b3f9023806853fbf |
| Source note | uspto-grants-2008_11 |