Methanesulfonyl chloride → HCID 69219450, compound

Participants

Reaction Steps

A mixture of Example 7C (30 mg, 0.11 mmol) and CH3SO2Cl (13 mg, 0.112 mmol) in pyridine (4 mL) was stirred overnight at room temperature. The excess pyridine was removed under reduced pressure and the residue was washed with hexanes and filtered. The filter cake was dried in a vacuum oven to provide the desired product. MS (DCI) m/e 338 (M+H)+, 355 (M+NH4)+.

Provenance & Evidence