HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azepane → HCID 69114582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azepane | HCID 8119 | — |
| Reactant | 2-Cyanobenzenesulfonyl Chloride | HCID 522347 | — |
| Reactant | HCID 69273622 | HCID 69273622 | — |
| Product | HCID 69114582 | HCID 69114582 | — |
Reaction Steps
A (125 mg) was prepared in two steps from 2-cyanobenzene-1-sulfonyl chloride (100 mg) and azepane in 82% overall yield following procedures analogous to those used in the preparation of 2-(aminomethyl)-N-tert-butyl-N-methylbenzenesulfonamide hydrochloride salt. LC-MS: 269.25 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456195B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-5cb3f5d846fd4fe6b1d8c5f2e3c85929 |
| Source note | uspto-grants-2008_11 |