HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 61287344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | 2-(Methylamino)ethanol | HCID 8016 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 61287344 | HCID 61287344 | 56.5% |
Reaction Steps
2-(Methylamino)-ethanol (1.0 g, 13.3 mmol), acetone (20 ml, 20 vol), 5M NaOH solution (3.19 ml, 1.2 eq.) and 1-bromo-3-chloropropane (6.28 g, 39.9 mmol, 3 eq.) were reacted together according to general procedure A to give the title compound (1.14 g, 55%) as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456164B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-3393ce48cbe146ebba018bda53b659c2 |
| Source note | uspto-grants-2008_11 |