HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11667281, compound → HCID 68578749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11667281 | HCID 11667281 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 68578749 | HCID 68578749 | 100% |
Reaction Steps
The title compound (1.05 g, 100%) was prepared from 4-{4-[(1-cyclobutyl-4-piperidinyl)oxy]phenyl}tetrahydro-2H-pyran-4-carbonitrile and lithium aluminium hydride similarly to the procedure used for intermediate 51. LRMS APCI+ m/z 345 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456164B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-cb295fd4a0fa46f596ac049a06dddd89 |
| Source note | uspto-grants-2008_11 |