huagongshe.com
HRID273005

反应详情

EQUATION

反应方程式

HRID 273005 的结构方程式

REACTANTS

反应物

3
结构：C1COCCN1
HCID8083

Morpholine

C4H9NO

结构：COc1ccc(C2(C(=O)O)CCOCC2)cc1
HCID969802

4-(4-methoxyphenyl)tetrahydro-2H-pyran-4-carboxylic acid

C13H16O4

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

PRODUCTS

生成物

1
结构：COc1ccc(C2(C(=O)N3CCOCC3)CCOCC2)cc1
HCID976657

未命名化合物

收率 87%

PROCEDURE

实验过程

The title compound (3.1 g, 87%) was prepared using 4-(4-methoxyphenyl)tetrahydro-2H-pyran-4-carboxylic acid, morpholine and O-(1H-benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate (TBTU) similarly to the procedure used for example 166. HRMS ESI+ m/z 306.1696 [MH]+.