反应详情

The title compound (2.42 g, 91%) was prepared using 4-{4-[(3-pyrrolidin-1-ylpropyl)thio]phenyl}tetrahydro-2H-pyran-4-carbonitrile and lithium aluminium hydride similarly to the procedure used for intermediate 51. LRMS APCI+ m/z 335 [MH]+. Microanalysis: Found: C, 64.08; H, 8.79; N, 7.447%. C19H30N2OS.0.33DCM requires C, 64.04; H, 8.52; N, 7.73%.