HuagongsheHuagongshe Chemistry Print Report · For research reference only
HC Yellow no. 13 → 2-[[2-Amino-4-(trifluoromethyl)phenyl]amino]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HC Yellow no. 13 | HCID 2799157 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-[[2-Amino-4-(trifluoromethyl)phenyl]amino]ethanol | HCID 21710172 | — |
Reaction Steps
2-{[2-nitro-4-(trifluoromethyl)phenyl]amino}ethanol (3.05 g, 12 mmol) was dissolved in THF (10 ml) and hydrogenated at 70 psi. After the removal of catalyst the product was obtained by evaporating the solvent and used for the next step (2.70 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07456293B2 |
| Source dataset | uspto-grants-2008_11 |
| ORD ID | ord-6a571cd67a9a4531aaa351bc25da194a |
| Source note | uspto-grants-2008_11 |