HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-benzylthiobenzimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-benzylthiobenzimidazole | HCID 416770 | 77.6% |
Reaction Steps
15 g of 2-mercaptobenzimidazole and 16.5 g of benzylbromide were dissolved in 50 ml of ethanol and the mixture was refluxed with a water bath for 5 hours. After cooling, the formed crystals were collected and recrystallized from ethanol to obtain 18 g of compound (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05387600 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-7175b79b224f4cfa82d7a772c722a4a5 |
| Source note | uspto-grants-1995_02 |