HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Ethyl cyclohexylamine → 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Ethyl cyclohexylamine | HCID 21609 | — |
| Reactant | 4-Chloro-3-nitrobenzophenone | HCID 41743 | — |
| Product | 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone | HCID 23342778 | — |
Reaction Steps
13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221739 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-84ea0d37cd7e4ceea09e7d996fe0f21e |
| Source note | uspto-grants-1980_09 |