Boron trifluoride → HCID 11073684, compound

Participants

Reaction Steps

43 g of boron trifluoride were passed into 200 ml of dimethyl carbonate under stirring at 25°-30° C. for 20 minutes. The resulting crystalline precipitate was filtered in dry nitrogen atmosphere, washed with pentane and dried under vacuum at room temperature to constant weight to give 98 g of dimethyl carbonate trifluoroborane, as white crystals.

Provenance & Evidence