Boron trifluoride → HCID 11073684, compound

HRID 273873Notes

Reaction equation

HRID 273873 reaction equation
[B:1]([F:4])([F:3])[F:2].[C:5](=[O:10])([O:8][CH3:9])[O:6][CH3:7]>>[F:2][B:1]([F:4])[F:3].[C:5](=[O:10])([O:8][CH3:9])[O:6][CH3:7]

Participants

3

Reactant 2

HCID 6356Boron trifluorideHCID 12021Dimethyl Carbonate

Product 1

HCID 11073684HCID 11073684, compound

Procedure

43 g of boron trifluoride were passed into 200 ml of dimethyl carbonate under stirring at 25°-30° C. for 20 minutes. The resulting crystalline precipitate was filtered in dry nitrogen atmosphere, washed with pentane and dried under vacuum at room temperature to constant weight to give 98 g of dimethyl carbonate trifluoroborane, as white crystals.

Workup

  1. filtrationThe resulting crystalline precipitate was filtered in dry nitrogen atmosphere
  2. washwashed with pentane
  3. customdried under vacuum at room temperature to constant weight

Sources & evidence

ORD record
ord-3fdcd326290e4611a123253507ca35f1
Source dataset
uspto-grants-1995_02
Patent number
US05387679

Reaction notes

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