HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 6-(Methylsulfinyl)imidazo[1,2-a]pyridine-2-carbamic acid, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 6-(Methylthio)imidazo[1,2-a]pyridine-2-carbamic acid, methyl ester | HCID 86737200 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 6-(Methylsulfinyl)imidazo[1,2-a]pyridine-2-carbamic acid, methyl ester | HCID 86737199 | — |
Reaction Steps
A suspension of 6-(methylthio)imidazo[1,2-a]pyridine-2-carbamic acid, methyl ester (prepared as described in Example 1) (0.447 mol) in 2700 ml of HOAc is treated dropwise with 535 ml of 30% H2O2. The suspension is stirred until a solution is obtained (~5 hours) and then poured into 8 l. of ice water. The product is collected by filtration and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221796 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-d25ac9d2d7974aa2ba67cdb206b026c0 |
| Source note | uspto-grants-1980_09 |