HRID274160

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6101

4-Methylbenzenesulfonic acid

C7H8O3S

HCID2736986

p-(Difluoromethoxy)benzaldehyde

C8H6F2O2

HCID21837878

Pentane-3,3-diol

C5H12O2

PRODUCTS

生成物

HCID19436343

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

17.2 g of p-difluoromethoxybenzaldehyde (commercially available from Fluorochem. Ltd. (GB)), 10.4 g of ethylpropanediol and 0.2 g of p-TsOH are heated to boiling for 2 hours in 100 ml of toluene. After evaporation of the solvent, the mixture is worked up as usual.

WORKUP

后处理

customAfter evaporation of the solvent