HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86748455, compound → HCID 86748454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86748455 | HCID 86748455 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86748454 | HCID 86748454 | — |
Reaction Steps
150 mg of (5-(4-cyanobenzylidene)-1-methyl-2,4-dioxoimidazolidin-3-yl)-acetyl-L-aspartyl-L-valine are dissolved in 40 ml of methanol. After addition of 50 mg of 10% strength Pd-on-charcoal, hydrogenation is carried out at room temperature for 12 hours, the catalyst is filtered off, the filtrate is concentrated and the product is freeze-dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389614 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-f3743934561c4955b75245b172847a5f |
| Source note | uspto-grants-1995_02 |