HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (5-(4-Cyanobenzylidene)-2,4-dioxoimidazolidin-3-yl)-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 53926892 | HCID 53926892 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | (5-(4-Cyanobenzylidene)-2,4-dioxoimidazolidin-3-yl)-acetic acid | HCID 54409679 | — |
Reaction Steps
0.4 g (1.1 mmol) of benzyl (5-(4-cyanobenzylidene)-2,4-dioxoimidazolidin-3-yl)-acetate are heated under reflux with 5 ml of 6N HCl and 5 ml of acetic acid for 30 minutes, the mixture is filtered hot and the filtrate is cooled. The product which has precipitated is filtered off with suction, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389614 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-9f7e358b7449475c9669d89d661311f6 |
| Source note | uspto-grants-1995_02 |