HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86748457, compound → HCID 86748456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86748457 | HCID 86748457 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86748456 | HCID 86748456 | — |
Reaction Steps
400 mg of (5-(4-cyanobenzylidene)-2,4-dioxoimidazolidin-3-yl)-acetyl-L-aspartyl-L-valine are dissolved in 60 ml of methanol. After addition of 50 mg of 10% strength Pd-on-charcoal, hydrogenation is carried out at room temperature for 12 hours, the catalyst is filtered off, the filtrate is concentrated and the product is freeze-dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389614 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-702cd760efef419a878094daa2c411db |
| Source note | uspto-grants-1995_02 |