1,3-Dibromopropane → Ethyl 5-bromo-2,2-diethylvalerate

HRID 274292Notes

Reaction equation

HRID 274292 reaction equation
[CH2:1]([CH:3]([CH2:9][CH3:10])[C:4]([O:6][CH2:7][CH3:8])=[O:5])[CH3:2].[Br:11][CH2:12][CH2:13][CH2:14]Br>>[Br:11][CH2:12][CH2:13][CH2:14][C:3]([CH2:9][CH3:10])([CH2:1][CH3:2])[C:4]([O:6][CH2:7][CH3:8])=[O:5]

Participants

3

Reactant 2

HCID 80011,3-DibromopropaneHCID 76326Ethyl 2-ethylbutyrate

Product 1

HCID 10849263Ethyl 5-bromo-2,2-diethylvalerate

Procedure

Using ethyl 2-ethylbutyrate and 1,3-dibromopropane, the same reaction as in Reference Example 16 was conducted to produce the title compound. b.p. 98°-102° C./0.3 mmHg

Workup

  1. customthe same reaction as in Reference Example 16

Sources & evidence

ORD record
ord-303828d9874944f69552c1a2e4c7233c
Source dataset
uspto-grants-1995_02
Patent number
US05389633

Reaction notes

Loading…