Dimethylamine, hydrochloride → 3-hydroxy-N,N-dimethylpropane-1-sulfonamide

HRID 274297Notes

Reaction equation

C([O:4][CH2:5][CH2:6][CH2:7][S:8](Cl)(=[O:10])=[O:9])(=O)C.Cl.[CH3:13][NH:14][CH3:15]>>[CH3:13][N:14]([CH3:15])[S:8]([CH2:7][CH2:6][CH2:5][OH:4])(=[O:10])=[O:9]

Participants

Reactant 2

HCID 10473Dimethylamine, hydrochloride

HCID 105842113-(Chlorosulfonyl)propyl acetate

Product 1

HCID 152348883-hydroxy-N,N-dimethylpropane-1-sulfonamide

Procedure

Using 3-acetoxypropane-1-sulfonyl chloride and dimethylamine hydrochloride, the same reaction as in Reference Example 44 and 46 was conducted to produce the title compound.

Workup

customthe same reaction as in Reference Example 44 and 46

Sources & evidence

ORD record: ord-9faa3e48529e44feb8d7722f3e24620c
Source dataset: uspto-grants-1995_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05389633

Reaction notes

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