HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → 3-(1-Methyl-4-piperazinylsulfonyl)-1-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 3-(Chlorosulfonyl)propyl acetate | HCID 10584211 | — |
| Product | 3-(1-Methyl-4-piperazinylsulfonyl)-1-propanol | HCID 15234889 | — |
Reaction Steps
Using 3-acetoxypropane-1-sulfonyl chloride and 1-methylpiperazine, the same reaction as in Reference Example 44 and 46 was conducted to produce the title compound. m.p. 90°-93° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05389633 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-8ae26d1d66354be29ec0dbb0f6315e72 |
| Source note | uspto-grants-1995_02 |