HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 23342828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 23342841 | HCID 23342841 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 23342828 | HCID 23342828 | — |
Reaction Steps
Add a solution of 0.75 g of acetyl chloride in 5 ml of benzene drop by drop to a solution of 1.9 g of the title compound of Example 22 and 1 g of triethylamine in 10 ml of benzene. After an hour concentrate the resulting product, take it up with water and diethyl ether, collect the organic phase and concentrate it to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221788 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-8cbc41c33a6a472cadf7e50e719973b3 |
| Source note | uspto-grants-1980_09 |