2-Chloropyrimidine → HCID 15239103, compound

HRID 274353Notes

Reaction equation

HRID 274353 reaction equation
[Na].[CH3:2][CH:3]([OH:17])[CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH:13]([CH3:16])[CH2:14][CH3:15])=[CH:8][CH:7]=1.Cl[C:19]1[N:24]=[CH:23][CH:22]=[CH:21][N:20]=1>>[CH3:2][CH:3]([O:17][C:19]1[N:24]=[CH:23][CH:22]=[CH:21][N:20]=1)[CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH:13]([CH3:16])[CH2:14][CH3:15])=[CH:8][CH:7]=1

Participants

4

Reactant 3

HCID 744042-ChloropyrimidineHCID 5360545SodiumHCID 15239095HCID 15239095, compound

Product 1

HCID 15239103HCID 15239103, compound

Procedure

In the same manner, the sodium salt of 1-methyl-2-[4-(1-methylpropoxy)phenoxy]ethanol and 2-chloropyrimidine are reacted together to give 2-{1-methyl-2-[4-(1-methylpropoxy)phenoxy]ethoxy}pyrimidine, MS m/e 320 (M+ +NH4).

Sources & evidence

ORD record
ord-29762d7cca414f409ddc7dcacfafd358
Source dataset
uspto-grants-1995_02
Patent number
US05389651

Reaction notes

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