HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-(4-Methylbenzyl)perhydroazepin-2-one → 2-(4-Methylbenzyl)azepane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-(4-Methylbenzyl)perhydroazepin-2-one | HCID 12349326 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 2-(4-Methylbenzyl)azepane | HCID 4239159 | — |
Reaction Steps
Using the mode of operation described in Example 52 obtain 1.6 g of the title compound as oil with a BP of 82° to 85° at 0.01 mm Hg from 2.8 of 7-(4-methylbenzyl)perhydroazepin-2-one and 0.5 of g lithium aluminum hydride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04221788 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-f00fcf268c734d1c997807c59e15a786 |
| Source note | uspto-grants-1980_09 |