Triethylamine → 2-(7-Methoxynaphthalen-1-yl)acetonitrile

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Triethylamine	HCID 8471	—
Edukt	Trifluoroacetic anhydride	HCID 9845	—
Edukt	2-(7-Methoxynaphthalen-1-yl)acetamide	HCID 15149127	—
Lösungsmittel	Tetrahydrofuran	HCID 8028	—
Produkt	2-(7-Methoxynaphthalen-1-yl)acetonitrile	HCID 11264068	—

Reaktionsschritte

The (7-methoxynaphth-1-yl)acetamide obtained in step E is suspended in 80 cm3 of anhydrous tetrahydrofuran. Triethylamine is added. The solution is cooled in an ice bath, and then trifluoroacetic anhydride is added dropwise, with magnetic stirring.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US05389683
Quelldatensatz	uspto-grants-1995_02
ORD ID	ord-2e97d8287bca467d8095a8a13555985c
Quellennotiz	uspto-grants-1995_02