HRID274760

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8471

Triethylamine

C6H15N

HCID9845

Trifluoroacetic anhydride

C4F6O3

HCID15149127

2-(7-Methoxynaphthalen-1-yl)acetamide

C13H13NO2

PRODUCTS

生成物

HCID11264068

7-Methoxy-1-naphthylacetonitrile

C13H11NO

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The (7-methoxynaphth-1-yl)acetamide obtained in step E is suspended in 80 cm3 of anhydrous tetrahydrofuran. Triethylamine is added. The solution is cooled in an ice bath, and then trifluoroacetic anhydride is added dropwise, with magnetic stirring.

WORKUP

后处理

temperatureThe solution is cooled in an ice bath