Ammonia → 7-Methoxy-1-naphthaleneethanamine

HRID 274761노트

반응식

HRID 274761 반응식
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH2:13][C:14]#[N:15])=[CH:5][CH:4]=1.N.[H][H]>C(O)C.[Ni]>[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH2:13][CH2:14][NH2:15])=[CH:5][CH:4]=1

참가 물질

6

반응물 3

HCID 222AmmoniaHCID 112640682-(7-Methoxynaphthalen-1-yl)acetonitrileHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 110526677-Methoxy-1-naphthaleneethanamine

시약·촉매·용매 2

HCID 935Nickel촉매HCID 702Ethanol용매

실험 절차

A solution of (7-methoxynaphth-1-yl)acetonitrile in ethanol saturated with ammonia is placed in an autoclave. Raney nickel and hydrogen are added under 300 atmospheres.

출처 및 근거

ORD 기록
ord-fa0208ca0a5442fb9bc1a72a5cacf334
출처 데이터셋
uspto-grants-1995_02
특허 번호
US05389683

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