HRID27477

反应详情

EQUATION

反应方程式

HRID 27477 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Potassium carbonate (7.75 g.) was added to a solution of 4-methyl-5-[(2-aminoethyl)thiomethyl]-imidazole dihydrochloride (14.6 g.) in water (120 ml.). The solution was stored at room temperature for 15 minutes, then evaporated to dryness, extracted with isopropyl alcohol and the extracts are concentrated to dryness to give 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole.

WORKUP

后处理

  1. customevaporated to dryness
  2. extractionextracted with isopropyl alcohol
  3. concentrationthe extracts are concentrated to dryness