HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178440675, compound → 1,2,3,4-Tetrahydroacridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178440675 | HCID 178440675 | — |
| Solvent | Phosphorus oxychloride | HCID 24813 | — |
| Product | 1,2,3,4-Tetrahydroacridine | HCID 155315 | — |
Reaction Steps
7-(1,1-Dimethylethyl)-9-hydroxy-1,2,3,4-tetrahydroacridine (9.46 g) was refluxed for 30 minutes in 50 ml of POCl3. The volatiles were evaporated and the residue was distributed between aqueous NH3 and Et2O. Concentration of the organic phase gave 8.24 g of 9-chloro-7-1,1-dimethylethyl)-1,2,3,4-tetrahydroacridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05391553 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-d49da7c79046488e9d1316a16e270795 |
| Source note | uspto-grants-1995_02 |