HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15239992, compound → methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15239992 | HCID 15239992 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | methyl 6-(N,N-dimethylamino)-3-hydroxypicolinate | HCID 15767145 | — |
Reaction Steps
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and was hydrogenated under normal pressure, after the reaction, the reaction product was filtrated and concentrated to obtain a crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05391537 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-d4b79056edcf4a36b03943e9afab1acc |
| Source note | uspto-grants-1995_02 |