HRID274884
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and was hydrogenated under normal pressure, after the reaction, the reaction product was filtrated and concentrated to obtain a crystal.
WORKUP
后处理
- customafter the reaction
- filtrationthe reaction product was filtrated
- concentrationconcentrated
- customto obtain a crystal