HRID274884

反应详情

EQUATION

反应方程式

HRID 274884 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2.3 g (8 mmol) of methyl 3-benzyloxy-6-(N,N-dimethylamino)picolinate and 0.3 g of 10% palladium carbon were added to 100 ml of ethyl acetate, and was hydrogenated under normal pressure, after the reaction, the reaction product was filtrated and concentrated to obtain a crystal.

WORKUP

后处理

  1. customafter the reaction
  2. filtrationthe reaction product was filtrated
  3. concentrationconcentrated
  4. customto obtain a crystal