HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 54027150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 54228721 | HCID 54228721 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54027150 | HCID 54027150 | — |
Reaction Steps
A mixture of 60.8 g (0.2 Mol) of N-trifluoroacetyl-4-nitro-phenylalanine, 250 ml of glacial acetic acid, 94 ml (1.0 Mol) of acetic anhydride and 10 g 10% palladium/charcoal is hydrogenated for 5 hours at 50° C. under 5 bars of hydrogen. The mixture is then suction filtered and the filtrate is evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05391556 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-e081c695b4ab4f49aedbfa7ac8ad69ee |
| Source note | uspto-grants-1995_02 |