HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 274960Generated: October 26, 2026
1,8-Naphthosultone → HCID 178428645, compound
https://huagongshe.com/reaction/274960
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,8-Naphthosultone | HCID 65744 | — |
| Reactant | HCID 178428665 | HCID 178428665 | — |
| Product | HCID 178428645 | HCID 178428645 | — |
Reaction Steps
Prepared from 1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethylamine and 1,8naphthalene sultone by heating to 100° C. for 30 minutes and subsequently heating to 140° C. for 20 minutes. After cooling, the product obtained is purified over a silica gel column (eluant: ethyl acetate/methanol=9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05391556 |
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| Source dataset | uspto-grants-1995_02 |
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| ORD ID | ord-c1a76724d6cd4cb5ae7c96342e548a00 |
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| Source note | uspto-grants-1995_02 |
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