HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indene → HCID 67740918, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indene | HCID 7219 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67740918 | HCID 67740918 | — |
Reaction Steps
50 ml of purified tetrahydrofuran (THF) was charged into a three-necked 300 ml flask, then 20 g of indene and 4 g of metal sodium were added, and reaction was allowed to take place at reflux for 4 hours. Thereafter, unreacted sodium was removed and then a 2 mols/l THF solution was prepared using the reaction product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05391660 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-22f2b04cc36444d7a32a382e9e2c289e |
| Source note | uspto-grants-1995_02 |