Indene → HCID 67740918, compound

HRID 274984Notes

Reaction equation

HRID 274984 reaction equation
[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[Na:10]>O1CCCC1>[Na:10].[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1

Participants

4

Reactant 2

HCID 7219IndeneHCID 5360545Sodium

Product 1

HCID 67740918HCID 67740918, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

50 ml of purified tetrahydrofuran (THF) was charged into a three-necked 300 ml flask, then 20 g of indene and 4 g of metal sodium were added, and reaction was allowed to take place at reflux for 4 hours. Thereafter, unreacted sodium was removed and then a 2 mols/l THF solution was prepared using the reaction product.

Workup

  1. customreaction
  2. temperatureat reflux for 4 hours
  3. customThereafter, unreacted sodium was removed
  4. customa 2 mols/l THF solution was prepared

Sources & evidence

ORD record
ord-22f2b04cc36444d7a32a382e9e2c289e
Source dataset
uspto-grants-1995_02
Patent number
US05391660

Reaction notes

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