Ethanesulfonyl chloride → HCID 60650381, compound

HRID 275299Notes

Reaction equation

[NH2:1][CH2:2][CH2:3][C:4]([O:6][CH3:7])=[O:5].[CH2:8]([S:10](Cl)(=[O:12])=[O:11])[CH3:9]>>[CH2:8]([S:10]([NH:1][CH2:2][CH2:3][C:4]([O:6][CH3:7])=[O:5])(=[O:12])=[O:11])[CH3:9]

Participants

Reactant 2

HCID 11667Ethanesulfonyl chloride

HCID 192794Methyl beta-alanate

Product 1

HCID 60650381HCID 60650381, compound

Procedure

N-(ethylsulfonyl)-β-alanine, methyl ester (21) was prepared from methyl β-alaninate and ethanesulfonyl chloride on a 32 mmol scale in the manner described in Example 13 above to yield 1.53 g (24%) of product.

Sources & evidence

ORD record: ord-3890ef0167e349eaaf0665f1907d3c53
Source dataset: uspto-grants-1995_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05393747

Reaction notes

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