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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 275302Generated: October 30, 2026

8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, hydrazide → HCID 86746507, compound

https://huagongshe.com/reaction/275302

Reaction equation

Participants

RoleNameHCIDCharge
Reactant8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, hydrazideHCID 13560461—
ReactantHCID 19800028HCID 19800028—
ProductHCID 86746507HCID 86746507—

Reaction Steps

8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, 2-[3-[(phenylsulfonyl)amino]-1-oxopropyl]hydrazide (24) was prepared from N-(phenylsulfonyl)-β-alanine, methyl ester (23), prepared as described above in Example 23, and 8-chlorodibenz[b,f][1,4]-oxazepine-10(11H)-carboxylic acid, hydrazide (1), prepared as described above in Example 1, on a two mmol scale in the manner described in Example 18 above to yield 0.44 g (44%) of product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05393747
Source datasetuspto-grants-1995_02
ORD IDord-f3472cf2df5f41aea97c1e87857e4626
Source noteuspto-grants-1995_02