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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 275322Generated: November 1, 2026

HCID 10496436, compound → HCID 10657146, compound

https://huagongshe.com/reaction/275322

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10496436HCID 10496436—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
ProductHCID 10657146HCID 10657146—

Reaction Steps

Hydrogenate cis-5,6a,7,8,9,9a-hexahydro-5-methyl-3-(phenylmethyl)cyclopenta[4,5]imidazo[2,1-b]purin-4-one (0.3 g=0.93 mmol) at room temperature/60 psi in EtOH (125 ml) containing 0.4 g Pearlman catalyst. Filter catalyst, remove solvent, and recrystallize to give the title compound as a white solid. FAB MS: M+1=232.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05393755
Source datasetuspto-grants-1995_02
ORD IDord-429e256a0d5a48f59c480e1055754172
Source noteuspto-grants-1995_02