HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10496436, compound → HCID 10657146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10496436 | HCID 10496436 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10657146 | HCID 10657146 | — |
Reaction Steps
Hydrogenate cis-5,6a,7,8,9,9a-hexahydro-5-methyl-3-(phenylmethyl)cyclopenta[4,5]imidazo[2,1-b]purin-4-one (0.3 g=0.93 mmol) at room temperature/60 psi in EtOH (125 ml) containing 0.4 g Pearlman catalyst. Filter catalyst, remove solvent, and recrystallize to give the title compound as a white solid. FAB MS: M+1=232.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05393755 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-429e256a0d5a48f59c480e1055754172 |
| Source note | uspto-grants-1995_02 |