HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 14969707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 6-Amino-3-benzyl-2-(methylsulfanyl)pyrimidin-4(3H)-one | HCID 20087830 | — |
| Product | HCID 14969707 | HCID 14969707 | — |
Reaction Steps
Reflux 6-amino-3-(phenylmethyl)-2-methylthiopyrimidin-4(3H)-one (2.5 g=10 mmol) in 40 ml 10% aqueous NaOH for four hours. Cool, acidify the solution and collect the precipitate. Water wash and dry to give the title compound, a white solid, EI MS: M+=217.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05393755 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-c7f84f230282458da550577707bb6e2e |
| Source note | uspto-grants-1995_02 |