HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 2-Chloro-1,7-bis(phenylmethyl)purin-6-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 1H-Purine-2,6-dione, 3,7-dihydro-1,7-bis(phenylmethyl)- | HCID 10914551 | — |
| Product | 2-Chloro-1,7-bis(phenylmethyl)purin-6-one | HCID 20087886 | — |
Reaction Steps
Treat 1,7-bis(phenylmethyl)purin-2,6-dione with POCl3 in accordance with Preparative Example 4, to give the title compound, an off-white solid, EI MS: M+=350.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05393755 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-970a631596fa446fa9adce628d74887a |
| Source note | uspto-grants-1995_02 |