HRID275395

反应详情

EQUATION

反应方程式

HRID 275395 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Under vigorous stirring 18.5 g of boron trifluoride etherate was added slowly to a solution of 60.6 g of 2,2-bis(4-fluorophenyl)oxirane in 450 ml of toluene. The mixture was washed twice with water, the solvent was evaporated and the residue was distilled to yield α-(4-fluorophenyl)-4-fluorobenzeneacetaldehyde.

WORKUP

后处理

  1. washThe mixture was washed twice with water
  2. customthe solvent was evaporated
  3. distillationthe residue was distilled