HRID275395
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Under vigorous stirring 18.5 g of boron trifluoride etherate was added slowly to a solution of 60.6 g of 2,2-bis(4-fluorophenyl)oxirane in 450 ml of toluene. The mixture was washed twice with water, the solvent was evaporated and the residue was distilled to yield α-(4-fluorophenyl)-4-fluorobenzeneacetaldehyde.
WORKUP
后处理
- washThe mixture was washed twice with water
- customthe solvent was evaporated
- distillationthe residue was distilled