HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → 2,2-Bis(4-fluorophenyl)acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | 2,2-Bis(4-fluorophenyl)oxirane | HCID 13983937 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,2-Bis(4-fluorophenyl)acetaldehyde | HCID 12549104 | — |
Reaction Steps
Under vigorous stirring 18.5 g of boron trifluoride etherate was added slowly to a solution of 60.6 g of 2,2-bis(4-fluorophenyl)oxirane in 450 ml of toluene. The mixture was washed twice with water, the solvent was evaporated and the residue was distilled to yield α-(4-fluorophenyl)-4-fluorobenzeneacetaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05393759 |
| Source dataset | uspto-grants-1995_02 |
| ORD ID | ord-585f1c1903ce4db29424e5e87439e085 |
| Source note | uspto-grants-1995_02 |