Methyl isothiocyanate → HCID 15230793, compound

Participants

Reaction Steps

To a solution of 0.500 g (0.0016 mole) of 2,6-bis (1,1-dimethylethyl) -4- [1- (hydroxyamino) ethyl ]phenol acetate is added 0.128 g (0.00175) of methyl isothiocyanate. The reaction mixture is stirred at room temperature for 18 hours and evaporated to near dryness. The residue is washed with Et2O and there is obtained 0. 300 g (55% ) white solid, m.p. 175°-175.5° C.

Provenance & Evidence