HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → ethyl N-(3,4-dimethoxybenzyl)-beta-alaninate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Veratrylamine | HCID 79832 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | ethyl N-(3,4-dimethoxybenzyl)-beta-alaninate | HCID 1908440 | — |
Reaction Steps
A mixture of 3,4-dimethoxy-benzylamine (100 g) and ethyl acrylate (65 ml) in ethanol (2L) and cylcohexane (1L) was stirred at room temperature for 20 hours then evaporated to give the title compound as a colourless oil (154 g). MS: 268 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06352977B1 |
| Source dataset | uspto-grants-2002_03 |
| ORD ID | ord-aa63fc6673fd43a498980b015f191263 |
| Source note | uspto-grants-2002_03 |