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HRID275888

反应详情

EQUATION

反应方程式

HRID 275888 的结构方程式

REACTANTS

反应物

2
结构：C=CC(=O)OCC
HCID8821

Ethyl acrylate

C5H8O2

结构：COc1ccc(CN)cc1OC
HCID79832

3,4-Dimethoxybenzylamine

C9H13NO2

PRODUCTS

生成物

1
结构：CCOC(=O)CCNCc1ccc(OC)c(OC)c1
HCID1908440

N-[(3,4-Dimethoxyphenyl)methyl]-β-alanine ethyl ester

C14H21NO4

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CCO
溶剂HCID702

Ethanol

C2H6O

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

A mixture of 3,4-dimethoxy-benzylamine (100 g) and ethyl acrylate (65 ml) in ethanol (2L) and cylcohexane (1L) was stirred at room temperature for 20 hours then evaporated to give the title compound as a colourless oil (154 g). MS: 268 [MH]+.

WORKUP

后处理

  1. customthen evaporated