HRID275956

反应详情

EQUATION

反应方程式

HRID 275956 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Paladium/carbon(Pd/C, 5%, 0.5 g) was added to a solution of 4-fluoro-2-methoxynitrobenzene (1.65 g, 9.6 mmol) in ethanol, which was then stirred for 1 hour under 30 psi of hydrogen pressure. The reaction mixture was filtered to remove paladium/carbon, and concentrated to give 1.35 g of the titled compound. (Yield 100%)

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered
  2. customto remove paladium/carbon
  3. concentrationconcentrated