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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 275956Erstellt: 25. Oktober 2026

5-Fluoro-2-nitroanisole → 4-Fluoro-2-methoxyaniline

https://huagongshe.com/reaction/275956

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5-Fluoro-2-nitroanisoleHCID 2779250—
EduktHCID 178418361HCID 178418361—
LösungsmittelEthanolHCID 702—
Produkt4-Fluoro-2-methoxyanilineHCID 13532228100%

Reaktionsschritte

Paladium/carbon(Pd/C, 5%, 0.5 g) was added to a solution of 4-fluoro-2-methoxynitrobenzene (1.65 g, 9.6 mmol) in ethanol, which was then stirred for 1 hour under 30 psi of hydrogen pressure. The reaction mixture was filtered to remove paladium/carbon, and concentrated to give 1.35 g of the titled compound. (Yield 100%)

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06352993B1
Quelldatensatzuspto-grants-2002_03
ORD IDord-0d55248ed97d4bf9b89af13e68247d2d
Quellennotizuspto-grants-2002_03