HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Fluoro-2-nitroanisole → 4-Fluoro-2-methoxyaniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Fluoro-2-nitroanisole | HCID 2779250 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 4-Fluoro-2-methoxyaniline | HCID 13532228 | 100% |
Reaktionsschritte
Paladium/carbon(Pd/C, 5%, 0.5 g) was added to a solution of 4-fluoro-2-methoxynitrobenzene (1.65 g, 9.6 mmol) in ethanol, which was then stirred for 1 hour under 30 psi of hydrogen pressure. The reaction mixture was filtered to remove paladium/carbon, and concentrated to give 1.35 g of the titled compound. (Yield 100%)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06352993B1 |
| Quelldatensatz | uspto-grants-2002_03 |
| ORD ID | ord-0d55248ed97d4bf9b89af13e68247d2d |
| Quellennotiz | uspto-grants-2002_03 |