Hydrogen Bromide → HCID 18316762, compound

HRID 275980Notes

Reaction equation

HRID 275980 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([CH2:6][CH2:7]O)=[CH:4][CH:3]=1.[BrH:11]>>[BrH:11].[Br:11][CH2:7][CH2:6][C:5]1[CH:9]=[CH:10][C:2]([NH2:1])=[CH:3][CH:4]=1

Participants

3

Reactant 2

HCID 260Hydrogen BromideHCID 669044-Aminophenethyl alcohol

Product 1

HCID 18316762HCID 18316762, compound

Procedure

To 4-aminophenethyl alcohol (25 g) was added 48% hydrobromic acid (250 ml), and the mixture was heated under reflux for 4 hours with stirring. After cooling, collection of the resulting precipitates by filtration gave 4-(2-bromoethyl)aniline hydrobromide (30.3 g).

Workup

  1. temperaturethe mixture was heated
  2. temperatureunder reflux for 4 hours
  3. temperatureAfter cooling
  4. customcollection of the resulting
  5. customprecipitates by filtration

Sources & evidence

ORD record
ord-027a6f8cf9374d9aa80d0ab52f08ffe0
Source dataset
uspto-grants-2002_03
Patent number
US06353025B1

Reaction notes

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